煤炭工程 ›› 2025, Vol. 57 ›› Issue (5): 92-98.doi: 10. 11799/ ce202505013

• 生产技术 • 上一篇    下一篇

难浮炼焦煤泥高效浮选分离工艺试验研究

陈辉, 何静谊, 张瑞, 等   

  1. 1. 太原煤炭气化(集团)有限责任公司选煤分公司
    2. 中国矿业大学(北京)
  • 收稿日期:2024-07-29 修回日期:2024-08-16 出版日期:2025-05-13 发布日期:2025-07-03
  • 通讯作者: 何静谊 E-mail:hejingyi0420@163.com

Experimental study on efficient flotation separation process of difficult-to-floate coking slime

  • Received:2024-07-29 Revised:2024-08-16 Online:2025-05-13 Published:2025-07-03

摘要:

针对常规浮选工艺处理微细粒含量极高煤泥时浮选精煤产率低,精煤灰分难以达到质量要求的问题,对龙泉4#入浮煤泥的浮选工艺进行了探索。 一粗一精二次浮选试验结果表明:高灰细泥夹带是造成精煤灰分偏高的主要原因,高剪切絮凝浮选可有效降低浮选精矿中的细泥夹带,最终确定高剪切絮凝浮选+一粗二精浮选工艺配以合理的浮选药剂制度可有效分选该煤泥;并采用激光粒度分析仪、接触角测量仪、扫描电镜等分析手段及煤颗粒与油滴碰撞概率的计算揭示了高剪切絮凝改善浮选效果的作用机理。研究结果表明:采用高剪切絮凝浮选+一粗二精浮选工艺,可使龙泉4#难浮煤泥的精煤灰分降至11.73%,产率达到50%左右,同时尾煤灰分提升至82.57%, 达到了分选要求。

关键词:

难浮煤泥 , 浮选工艺 , 高剪切 , 絮团 , 多段浮选

Abstract: In order to solve the problems of low concentrate yield and high ash content of concentrate which can not reach the qualified quality requirements (ash content of concentrate <12%) by conventional flotation process for Longquan 4# floating slime, the multi-stage flotation process was explored. The "one rougher, one cleaner" two-stage flotation tests revealed that the entrainment of high-ash fine slimes led to elevated ash content in the concentrate. Due to the high-shear flocculation flotation demonstrated a significant improvement in reducing fine slime entrainment, the "high-shear flocculation flotation +one rougher , two cleaner" flotation process combined with a reasonable flotation reagent system was adopted. The mechanisms underlying the improvement in flotation efficiency due to high-shear flocculation were analyzed using laser particle size analyzer, contact angle measuring instrument, scanning electron microscopy, and calculations of the collision probability between coal particles and oil droplets. The results indicated that using the flotation process of " high-shear flocculation flotation +one rougher, two cleaner ", the concentrate ash content of Longquan 4# difficult-to-floate coking slime can be reduced to 11.73%, the concentrate recovery rate reached approximately 50%, and the tail coal ash content can be increased to 82.57%. Both the concentrate and the tail coal index can meet the requirements of coal preparation plant.

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