煤炭工程 ›› 2021, Vol. 53 ›› Issue (4): 158-161.doi: 10.11799/ce202104032

• 研究探讨 • 上一篇    下一篇

海石湾煤制备超纯煤磨矿试验研究

王枭,赵世永   

  1. 西安科技大学
  • 收稿日期:2020-04-24 修回日期:2020-07-17 出版日期:2021-04-20 发布日期:2021-05-17
  • 通讯作者: 赵世永 E-mail:zhaoshiyong9@163.com

Feasibility test of preparation of ultrapure coal from haishiwan coal

  • Received:2020-04-24 Revised:2020-07-17 Online:2021-04-20 Published:2021-05-17

摘要: 超纯煤制备是煤炭高价值利用的基础。海石湾煤-1.4g/cm浮煤灰分低,产率大,具备制备超纯煤的物质条件。通过对灰分低于3%的低灰煤进行X射线衍射(XRD)及显微分析,研究低灰煤中的杂质矿物组成及赋存形态。在此基础上进行磨矿方式选择试验和磨矿时间、级配及分散剂等磨矿条件试验。试验发现:在同等条件下,湿法磨矿效果优于干法磨矿|当磨矿介质粒径组成越小、磨矿时间越长时,磨矿效果越好|添加0.55%六偏磷酸钠作分散剂,磨矿级配质量比取30mm∶25mm∶20mm∶15mm= 39.11%∶23.57%∶18.82%∶18.50%,湿磨4h时,煤粒与无机杂质矿物已基本解离。在此条件下进行浮选试验,浮选精煤产率为19.08%,灰分为0.88%。

关键词: 超纯煤, 磨矿方式, 磨矿时间, 级配, 分散剂

Abstract: The preparation of pure low ash coal ultra-pure coal is the foundation of coal high value-added processing conversion and utilization. Low ash content and high yield of -1.4 g/cm3 haishiwan floating coal has the material conditions for the preparation of ultra-pure coal low ash pure coal. The composition and occurrence form of impurity minerals in low ash coal were studied by X-ray diffraction (XRD) and microscopic analysis of low ash coal with ash content less than 3%.It is found that the low-ash coal with ash content less than 3% can be obtained by gravity separation of haishiwan raw coal through the analysis of sieve floating-settling experiment. On this basis, grinding experiments are carry out under such conditions as selection of grinding method, grinding time, gradationmedium ratio and dispersing agent. The results show that wet grinding is better than dry grinding under the same conditions. When the particle size composition of grinding medium is smaller and the grinding time is longer, the grinding effect is better. With the addition of 0.55% sodium hexametaphosphate as dispersant, the mass ratio was 39.11%:23.57%:18.82%:18.50% when the diameter ratio of the grinding medium grinding gradation was φ30mm: φ25mm: φ20mm: φ15mm, wet milling for 4h and. At this time, the coal particles had been basically dissociated from the inorganic impurities. In this case, The the yield of cleaned coal was 19.08% and the ash content was only 0.88% by flotation of wet grinding of mineral.