煤炭工程 ›› 2014, Vol. 46 ›› Issue (5): 107-109.doi: 10.11799/ce201405035

• 研究探讨 • 上一篇    下一篇

宝日希勒褐煤半焦的浮选试验研究

张仲玲1,马力强2,于跃先1   

  1. 1. 中国矿业大学(北京)
    2. 中国矿业大学(北京)化学与环境工程学院
  • 收稿日期:2013-06-12 修回日期:2013-07-12 出版日期:2014-05-15 发布日期:2014-05-10
  • 通讯作者: 张仲玲 E-mail:zzl19890814@yeah.net

Flotation experimental study on Baorixile semi-coke of the lignite

  • Received:2013-06-12 Revised:2013-07-12 Online:2014-05-15 Published:2014-05-10

摘要:

摘要:对褐煤和褐煤半焦进行工业分析、元素分析,发现低温热解提质后褐煤中的有机质成分和煤化程度都发生了变化;通过对比褐煤和褐煤半焦的红外光谱,发现褐煤半焦中的亲水性官能团主要为羟基、氢键、胺基和醚等,且其含量要小于在褐煤中的含量;对褐煤半焦进行粒度分析和浮选试验,捕收剂采用0#柴油、煤油、ZS和它们的两两组合,发现组合药剂制度的浮选效果优于单纯的药剂制度,但无论采用哪种药剂制度,褐煤半焦的药剂消耗量都巨大,精煤灰分偏高。并对药剂消耗量大的原因进行了分析,认为半焦中较高的孔隙度是主导因素。

关键词: 关键词:褐煤, 半焦, 红外光谱, 复合药剂, 孔隙度

Abstract:

By implementing industrial analysis and elemental analysis of lignite and semi-coke of lignite,we could easily find organic ingredients and coalification of lignite have taken great places after low temperature pyrolysis upgrading technology.Their comparison of infrared spectroscopy showed that the main hydrophilic functional groups in semi-coke included –OH,–H,–NH and –O– ect.Their contents were lower than in lignite.Carried on particle size analysis and flotation experiments of semi-coke,adopted 0#diesel,kerosene,ZS and their combination,the results showed that flotation effect was better when using complex flotation reagents than single reagent.But no matter which kind of reagent institution was adopted,reagents consumption were both enormous,as well as the high ash of concentrate.By means of analyzing the reasons of enormous reagents consumption,we could drow the conclusion that high degree of porosity was the dominant factor.

Key words: Key words:lignite, semi-coke, infrared spectroscopy, complex flotation reagents, degree of porosity

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